Latest Headlines

Identification and Characterization of Polyphenolic Antioxidants

Dr Per Sjöberg from the Department of Physical and Analytical Chemistry at Uppsala University in Sweden has demonstrated that electrochemistry (EC) coupled to liquid chromatography (LC) and electrospray ionization tandem mass spectrometry (LC/EC/ESI-MS/MS) can be used to rapidly obtain information about the antioxidant activity

Influence of Storage Conditions on Aroma Compounds in Coffee Pads by Using Static Headspace GC-MS

Dr Bart van der Bruggen and a team from the Department of Chemical Engineering, KU Leuven and PerkinElmer, Belgium, employed static headspace gas chromatography coupled to mass spectrometry (SHGC–MS) to identify aroma compounds in coffee pad powder.

Understanding protein phosphorylation with nano-ultra performance liquid chromatography-tandem mass spectrometry

Professor Wolf Lehmann, from Molecular Structure Analysis at the German Cancer Research Center (DKFZ) Heidelberg, Germany, conducted a study to characterize in detail the in vitro phosphorylation of the recombinant Plasmodium falciparum protein GAP45 by a kinase from the same organism.

Detection of human bladder cancer in human by LC-MS analysis of urine

The current use of cystoscopy for screening and detecting bladder cancer is invasive and expansive. Various urine-based biomarkers have been used for this purpose with limited success.

RPLC enantioresolution of six ß -blockers using 12 CDRs

Twelve chiral derivatizing reagents (CDRs) were synthesized by substituting one of the fluorine atoms in 1,5-difluoro-2,4-dinitrobenzene (DFDNB) with three optically pure amines [(R)-(-)-1-cyclohexylethylamine, (+)-dehydroabietylamine and (S)-(-)- ,4-dimethylbenzylamine], six amino acid amides [L-Ala-NH2, L-Phe-NH2, L-Val-NH2, L-Leu-NH2, L-Met-NH2 and D-Phg-NH2] and three amino acids [L-Ala, L-Val and L-Leu]. The work was led by Professor Ravi Bhushan from the Department of Chemistry at the Indian Institute of Technology Roorkee in India and documented in Biomedical Chromatography [23 (12) 1291 – 1299 (2009)].

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Simple-to-use slide-by-slide video presentations with instructional voiceover, together with a comprehensive handout supporting the learning experience.
 Fundamentals of
Gradient HPLC

Performance Qualification
of HPLC Equipment

Introduction to LC-MS
and LC-MS/MS

 HPLC Troubleshooting &
Preventive Maintenance
Session 1: Principles of
HPLC Troubleshooting


Session 2: HPLC Pumps
& Autosamplers


Session 3: Physical Problems
with HPLC Columns


Session 4: Chemical Problems
with HPLC Columns


Session 5: HPLC Detectors

Session 6: Quantification, Integration
and Data Systems


  


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